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ILNAS-EN 14105:2011 Edition 04/2011
Fat and oil derivatives - Fatty Acid Methyl Esters (FAME) - Determination of free and total glycerol and mono-, di-, triglyceride contents
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Abstract

The purpose of this European Standard is to determine the free glycerol and residual mono-, di- and triglyceride contents in fatty acid methyl esters (FAME) intended for addition to mineral oils. The total glycerol content is then calculated from the obtained results. This method is the reference method for the determination of the free glycerol content. Under the conditions described, the quantification limits are 0,001 % (m/m) for free glycerol, 0,10 % (m/m) for all glycerides (mono-, di- and tri-). This method is suitable for FAME prepared from rapeseed, sunflower, soybean, palm, animal oils and fats and mixture of them. It is not suitable for FAME produced from or containing coconut and palm kernel oils derivatives because of overlapping of different glyceride peaks. NOTE For the purposes of this European Standard, the term "% (m/m)" is used to represent respectively the mass fraction. WARNING - The use of this method may involve hazardous equipment, materials and operations. This method does not purport to address to all of the safety problems associated with its use, but it is the responsibility of the user to search and establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

Status

Standard - Superseded

Origin

Technical Committee :
CEN/TC 307 : Oilseeds, vegetable and animal fats and oils and their by-products - Methods of sampling and analysis

Implementation

start of the vote on the project    17/09/2009   date of ratification (dor)    10/03/2011
end of the vote on the project    17/03/2010   date of anouncement (doa)    31/07/2011
start of the vote on the final project    09/12/2010   date of publication (dop)    31/10/2011
end of the vote on the final project    09/02/2011   date of withdrawal (dow)    31/10/2011


Publication Official Journal
of the Grand-Duchy of Luxembourg
05/01/2012
Reference Mémorial A N° 2

Relations

Evolutions
ILNAS-EN 14105:2020

Relations to older standards
ILNAS-EN 14105:2003

International Classification for Standards (ICS codes) :

67.200.10 : Animal and vegetable fats and oils

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